Synthesis of Pinacol 4-Hydroxyphenyl Boronate

  • Synthesis of Pinacol 4-Hydroxyphenyl Boronate 01/21/2019

    Pinacol 4-Hydroxyphenyl Boronate was synthesised in 28.2% overall yield from 4-bromophenol by protection 

    with t-butyldimethylsilyl chloride,Grignard reaction and reaction with B(OCH3)3 to afford dimethyl 

    t-butyldimethylsilyloxyphenyl boronate followed by ester exchange with pinacol and then deprotection.


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